
Conical Disc Centrifuge / De laval Clarifier - Pharmaceutical Engineering B. Pharm Third Semester PDF Notes
Conical Disc Centrifuge / De laval Clarifier
Conical Disc Centrifuge
As it is a clarified, solids or immiscible liquids are present in low concentration in the feed complete clarification of the feed is possible by centrifugal means
Principle
• It is a sedimentation centrifuge
• The separation is based on the difference in the densities between the phases under the influence of centrifugal force
• In this, a number of cone shaped plates are attached to a central shaft (which has the provision for feed) at different elevations
• During centrifugation, the dense solids are thrown outwards to the underside of the cone shaped casing, while the lighter clarified liquid passes over the bowl and recovered from the top of the cone
Construction
• The construction of a conical disc centrifuge is shown in figure
• It construction of a shallow form of bowl contacting a series of conical disc are made up of a thin sheet of metal or plastic separated by narrow spaces
• Matching hole in the disc (above half way between the axis and the wall of the bowl) from channel through which the liquid passes
• A concentric tube is placed surrounding the central drive shaft
Working• Centrifuge is allowed to rotate.
• Low speed and short time of centrifugation is sufficient to give high degree of clarification
• The feed is introduced through the concentric tube surrounding the shafts
• The feed flow down and enters in to the space between the discs (show by the narrows)
• During centrifugation, the liquid flow in to the channel (holes at the centre of disc) and upward past the discs
• These substances move along the surfaces of the discs to the limits of the inner and outer layers
• The solids and heavy liquids are thrown outward and move underside of the discs
• Then the solids deposit at the bottom of the cone, which is removed intermittently
• The lighter liquid moves to the upper side of the discs
• The liquid raises to the top and escapes from the outlet
Uses
• Two immiscible liquids can be easily separated by a continuous process after liquid/liquid extraction as in case of manufacture of antibiotics
• Suspensions containing low concentration of solids can be separated quickly. Solids that are gelatinous are slimy can be separated by disc cone centrifuge. Such substances may plug the filter in the other methods
• Starch is collected after washing and purification stages
• In the manufacture of insulin, the liquor is clarified to remove the precipitated proteins
• Concentration of one fluid phase is possible as in the separation of cream from milk, concentration of rubber latex, removing solids from lubricating oils, inks and beverages
Advantages
• Conical disk centrifuges are compact occupying a very small space
• The separating efficiency is very high, so that the particle are deposited very rapidly. It is suitable, if the sediment is a fluid deposit or sludge
• By controlling the speed of rotation and rate of flow, particle are separated intotwo size fractions
Disadvantages
• The construction of a conical disc centrifuge is complicated
• Its capacity is limited
• It is not suitable if the sediment of solid forms a hard cake
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